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Karl Fischer Titrator, Volumetric and Coulometric

Karl Fischer titrator for water content that runs both volumetric and coulometric titration on one instrument, with a separate cell for each so trace and percent-level moisture can be handled.

Typical applications

  • Water content in solvents and oils
  • Moisture in active pharmaceutical ingredients and formulations
  • Moisture in foods and edible oils
  • Trace moisture in fine chemicals
  • Moisture in plastics and powders

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Worth knowing before you order

This is the first question to settle, and this model answers it both ways: it does volumetric and coulometric Karl Fischer titration on one chassis, with a volumetric titration cell and a coulometric electrolytic cup supplied together. Coulometric is the trace-moisture technique — the diaphragm generator cell and the micro cup are for samples at ppm level, where iodine is generated electrochemically and no titrant titre has to be maintained. Volumetric, using the 10 ml burette and a titrant of known titre, is for higher water contents; the printed volumetric range of 0.1 mg to 250 mg of water is the figure to size your sample against. The catalogue prints the coulometric range as '10µg ~ 20mA'; the upper figure is a current, not a mass, so only the 10 µg lower limit is reproduced here and the upper limit should be obtained in writing. Karl Fischer reagent, working medium, molecular sieve and drying-tube desiccant are consumables and none are listed. The 200-set memory is described as GLP-compliant; that compliance rests on the user's own procedures and records.

Specification

Technical specification for Karl Fischer Titrator, Volumetric and Coulometric
Quantity measuredWater (moisture) content
ModesVolumetric titration and coulometric titration
Volumetric titration range0.1 mg to 250 mg water
Volumetric polarisation current accuracy1 µA ± 0.2 µA, 50 µA ± 10 µA
Volumetric repeatability± 0.5%
Volumetric burette10 ml burette device
Coulometric titration range, lower limit10 µg (upper limit not usable as printed — see note)
Coulometric electrolytic current10 mA, 20 mA, 50 mA, 100 mA
Coulometric accuracy± (5% + 3) µg
Coulometric repeatability≤ 3%
Generator cellWith diaphragm
Drift correctionAutomatic or manual background drift correction
Reagent handlingAuto-filling, auto-purging and auto-mixing
Units, volumetricmg, mg/L, %, ppm
Units, coulometricµg, mg, %, ppm, mg/L, µg/mL
DisplayLCD, titration curve and results shown
Memory200 titration data sets
InterfaceRS232C
Power supplyAC 220 V / 50 Hz
Packing dimensions (L x W x H)535 x 500 x 480 mm
Gross weight13 kg

Support available

  • Installation & commissioning
  • Calibration
  • Validation & qualification (IQ/OQ/PQ)
  • Operator training
  • Annual maintenance contract
  • Spares & consumables

Calibration is arranged through NABL-accredited laboratories under the relevant scope. We state the scope and the certificate number on the quotation — see what accreditation actually covers.

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